a)
$2Al + 3H_2SO_4 \to Al_2(SO_4)_3 + 3H_2$
$Fe + H_2SO_4 \to FeSO_4 + H_2$
b)
Gọi $n_{Al} = a(mol) ; n_{Fe} = b(mol) \Rightarrow 27a + 56b = 0,83(1)$
Theo PTHH, $n_{H_2} = 1,5a + b = \dfrac{0,56}{22,4} = 0,025(2)$
Từ (1)(2) suy ra a = b = 0,01
$\%m_{Al} = \dfrac{0,01.27}{0,83}.100\% = 32,5\%$
$\%m_{Fe} = 100\% - 32,5\% = 67,5\%$